bis(dimethoxyboryl)phenylmethane

Base Information

• Chemical Name: bis(dimethoxyboryl)phenylmethane
• CAS No.: 17936-83-3
• Molecular Formula: C₁₁H₁₈B₂O₄
• Molecular Weight: 235.884
• Mol file: 17936-83-3.mol

Synonyms:

Chemical Property of bis(dimethoxyboryl)phenylmethane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of bis(dimethoxyboryl)phenylmethane

There total 2 articles about bis(dimethoxyboryl)phenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzylidene dichloride (98-87-3) + chlorodimethoxyborane (868-81-5) → bis(dimethoxyboryl)phenylmethane (17936-83-3)

Guidance literature:

Multistep reaction; (i) Li, hexane, THF, (ii) (heating);

DOI:10.1021/ja01010a057

Reference yield:

benzylidene dichloride (98-87-3) + Trimethyl borate (121-43-7,63156-11-6) → bis(dimethoxyboryl)phenylmethane (17936-83-3)

Guidance literature:

Multistep reaction; (i) BCl₃, (ii) /BRN= 1099407/, Li, hexane, THF;

DOI:10.1016/S0022-328X(00)80082-0

Reference yield:

bis(dimethoxyboryl)phenylmethane (17936-83-3) + trimethyleneglycol (504-63-2) → C6H5CH(B(OCH2)2CH2)2 (78782-25-9)

Guidance literature:

In tetrahydrofuran; overnight at 25 °C; evapn., recrystn. (ether, pentane), elem. anal.;

upstream raw materials:

benzylidene dichloride

Trimethyl borate

chlorodimethoxyborane

Downstream raw materials:

C₆H₅CH(B(OCH₂)2CH₂)2