n-(2,2,2-Trichloro-1-phenylethyl)benzamide

Base Information

Chemical Name:n-(2,2,2-Trichloro-1-phenylethyl)benzamide
CAS No.:60721-37-1
Molecular Formula:C15H12 Cl3 N O
Molecular Weight:328.625
Hs Code.:
NSC Number:143308
ChEMBL ID:CHEMBL1547508

Synonyms:n-(2,2,2-trichloro-1-phenylethyl)benzamide;60721-37-1;N1-(2,2,2-trichloro-1-phenylethyl)benzamide;NSC143308;MLS000389698;CHEMBL1547508;HMS2512B19;STL483210;AKOS001025548;AKOS016322236;NSC-143308;SMR000255972;Z56755682;F0757-0023

Suppliers and Price of n-(2,2,2-Trichloro-1-phenylethyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of n-(2,2,2-Trichloro-1-phenylethyl)benzamide

Chemical Property:

Vapor Pressure:2.76E-09mmHg at 25°C
Boiling Point:477.6°C at 760 mmHg
Flash Point:242.6°C
Density:1.358g/cm³
XLogP3:4.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:326.998447
Heavy Atom Count:20
Complexity:318

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(C(Cl)(Cl)Cl)NC(=O)C2=CC=CC=C2

Technology Process of n-(2,2,2-Trichloro-1-phenylethyl)benzamide

There total 5 articles about n-(2,2,2-Trichloro-1-phenylethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 98-88-4
benzoyl chloride

: 60721-42-8
2,2,2-Trichloro-1-phenyl-ethylamine; hydrochloride

: 60721-37-1
N-(2,2,2-trichloro-1-phenylethyl)benzamide

Guidance literature:: In benzene; for 4h; Heating;

Reference yield: 50.0%

: N-(2,2,2-trichloro-1-phenylethyl)benzimidoyl chloride

: 60721-37-1
N-(2,2,2-trichloro-1-phenylethyl)benzamide

Guidance literature:: With silica gel;
DOI:10.1021/acs.joc.8b01406

Reference yield:

: (Z)-3,3,3-trichloro-1,2-diphenylpropan-1-one oxime

: 60721-37-1
N-(2,2,2-trichloro-1-phenylethyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus pentachloride / benzene / 24 h / 20 °C

2: silica gel

With phosphorus pentachloride; silica gel; In benzene; 1: |Beckmann Rearrangement;
DOI:10.1021/acs.joc.8b01406