2,5-bis(thiolatomethyl)-1,4-dioctyloxybenzene

Base Information

• Chemical Name: 2,5-bis(thiolatomethyl)-1,4-dioctyloxybenzene
• CAS No.: 1313052-70-8
• Molecular Formula: C₂₄H₄₂O₂S₂
• Molecular Weight: 426.728
• Mol file: 1313052-70-8.mol

Synonyms:

Chemical Property of 2,5-bis(thiolatomethyl)-1,4-dioctyloxybenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-bis(thiolatomethyl)-1,4-dioctyloxybenzene

There total 6 articles about 2,5-bis(thiolatomethyl)-1,4-dioctyloxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-bis(octyloxy)benzene (67399-94-4) → 2,5-bis(thiolatomethyl)-1,4-dioctyloxybenzene (1313052-70-8)

Guidance literature:

Multi-step reaction with 4 steps

1: acetic acid

2: hydrogen bromide / acetic acid / 3 h / 80 °C

3: 12 h / 110 °C

4: sodium hydroxide / 4 h / 115 °C

With hydrogen bromide; acetic acid; sodium hydroxide; In acetic acid;

DOI:10.1021/jacs.7b06201

Reference yield:

C24H42O4 (444308-65-0) → 2,5-bis(thiolatomethyl)-1,4-dioctyloxybenzene (1313052-70-8)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogen bromide / acetic acid / 3 h / 80 °C

2: 12 h / 110 °C

3: sodium hydroxide / 4 h / 115 °C

With hydrogen bromide; sodium hydroxide; In acetic acid;

DOI:10.1021/jacs.7b06201

Reference yield:

C26H46N4O2S2*2BrH → 2,5-bis(thiolatomethyl)-1,4-dioctyloxybenzene (1313052-70-8)

Guidance literature:

With sodium hydroxide; at 115 ℃; for 4h;

DOI:10.1021/jacs.7b06201

upstream raw materials:

1,4-bis(bromomethyl)-2,5-bis(octyloxy)benzene

hydroquinone

1-bromo-octane

1,4-bis(octyloxy)benzene