1-Methyl-3-((1-methyl-4-nitro-1H-imidazol-2-yl)methylene)-2-pyrrolidinone

Base Information

Chemical Name:1-Methyl-3-((1-methyl-4-nitro-1H-imidazol-2-yl)methylene)-2-pyrrolidinone
CAS No.:123794-13-8
Molecular Formula:C₁₀H₁₂N₄O₃
Molecular Weight:236.23
Hs Code.:
Mol file:123794-13-8.mol

Synonyms:BRN 4814183;1-Methyl-3-((1-methyl-4-nitro-1H-imidazol-2-yl)methylene)-2-pyrrolidinone;2-Pyrrolidinone, 1-methyl-3-((1-methyl-4-nitro-1H-imidazol-2-yl)methylene)-;123794-13-8;LS-138900

Suppliers and Price of 1-Methyl-3-((1-methyl-4-nitro-1H-imidazol-2-yl)methylene)-2-pyrrolidinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 1-Methyl-3-((1-methyl-4-nitro-1H-imidazol-2-yl)methylene)-2-pyrrolidinone

Chemical Property:

Vapor Pressure:1.66E-10mmHg at 25°C
Boiling Point:509.7°C at 760 mmHg
Flash Point:262°C
Density:1.44g/cm³
XLogP3:0.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:236.09094026
Heavy Atom Count:17
Complexity:376

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CCC(=CC2=NC(=CN2C)[N+](=O)[O-])C1=O
Isomeric SMILES:CN1CC/C(=C/C2=NC(=CN2C)[N+](=O)[O-])/C1=O

Technology Process of 1-Methyl-3-((1-methyl-4-nitro-1H-imidazol-2-yl)methylene)-2-pyrrolidinone

There total 2 articles about 1-Methyl-3-((1-methyl-4-nitro-1H-imidazol-2-yl)methylene)-2-pyrrolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 118467-52-0
2-chloromethyl-1-methyl-4-nitro-1H-imidazole

: sel de lithium de la 1-methyl 3-nitropyrrolidin-2-one

: 138745-06-9,123794-13-8
1-methyl 2-(1-methyl pyrrolidin-2-one 3-ylidenemethyl) 4-nitroimidazole

Guidance literature:: With tetrabutylammomium bromide; In water; toluene;
DOI:10.1016/0223-5234(91)90118-7

Reference yield:

: 872-50-4,26138-58-9
1-methyl-pyrrolidin-2-one

: 138745-06-9,123794-13-8
1-methyl 2-(1-methyl pyrrolidin-2-one 3-ylidenemethyl) 4-nitroimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA, 2.) nC₃H₇ONO₂ / 1.) THF, hexane, 0 deg C, 30 min, 2.) THF, hexane, -25 deg C, 1.5 h

2: 70 percent / Bu₄NBr / H₂O; toluene

With propyl nitrate; tetrabutylammomium bromide; lithium diisopropyl amide; In water; toluene;
DOI:10.1016/0223-5234(91)90118-7