Pd2[μ-(C6F4)PPh2]2(μ-O2CCF3)2

Base Information

• Chemical Name: Pd2[μ-(C6F4)PPh2]2(μ-O2CCF3)2
• CAS No.: 919537-00-1
• Molecular Formula: C₄₀H₂₀F₁₄O₄P₂Pd₂
• Molecular Weight: 1105.36

Synonyms:

Chemical Property of Pd2[μ-(C6F4)PPh2]2(μ-O2CCF3)2

Chemical Property:

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Technology Process of Pd2[μ-(C6F4)PPh2]2(μ-O2CCF3)2

There total 1 articles about Pd2[μ-(C6F4)PPh2]2(μ-O2CCF3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

[Pd[μ-(C6F4)PPh2](μ-Br)]4 + silver trifluoroacetate (2966-50-9) → Pd2[μ-(C6F4)PPh2]2(μ-O2CCF3)2 (919537-00-1)

Guidance literature:

In dichloromethane; acetic acid; Pd-complex suspended in CH2Cl2-acetic acid, Ag-salt added, refluxed for 24 h in absence of light, cooled to room temp.; diluted with Et2O, passed through silica column, solvent removed under vac., ppt. extd. with Et2O, hexane added, solvent removed under vac.; elem. anal.;

DOI:10.1039/b609829k

upstream raw materials:

silver trifluoroacetate

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