C₂₃H₂₄N₂O₄S

Base Information

Chemical Name:C₂₃H₂₄N₂O₄S
CAS No.:1354817-71-2
Molecular Formula:C₂₃H₂₄N₂O₄S
Molecular Weight:424.521
Hs Code.:

C<sub>23</sub>H<sub>24</sub>N<sub>2</sub>O<sub>4</sub>S

Synonyms:

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Chemical Property of C₂₃H₂₄N₂O₄S

Chemical Property:

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Technology Process of C₂₃H₂₄N₂O₄S

There total 6 articles about C₂₃H₂₄N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354808-43-7
3-(4-bromophenyl)-3-o-tolylpropanoic acid

: 1354817-70-1
C₂₃H₂₄N₂O₄S

: 1354817-71-2
C₂₃H₂₄N₂O₄S

Guidance literature:: Multi-step reaction with 6 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / N,N-dimethyl-formamide

2: n-butyllithium / tetrahydrofuran / -78 °C

3: hydrogenchloride; water / 1,4-dioxane / 1.5 h / 100 °C

4: potassium carbonate / N,N-dimethyl acetamide

5: L-proline; copper(l) iodide; sodium hydroxide / dimethyl sulfoxide

6: hydroxylamine hydrochloride; sodium acetate / ethanol; water / Reflux

With hydrogenchloride; copper(l) iodide; n-butyllithium; hydroxylamine hydrochloride; water; sodium acetate; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; L-proline; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl acetamide; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.017

Reference yield:

: 1354810-21-1
(R)-3-(4-bromo-phenyl)-N-methoxy-N-methyl-3-o-tolyl-propionamide

: 1354817-70-1
C₂₃H₂₄N₂O₄S

: 1354817-71-2
C₂₃H₂₄N₂O₄S

Guidance literature:: Multi-step reaction with 5 steps

1: n-butyllithium / tetrahydrofuran / -78 °C

2: hydrogenchloride; water / 1,4-dioxane / 1.5 h / 100 °C

3: potassium carbonate / N,N-dimethyl acetamide

4: L-proline; copper(l) iodide; sodium hydroxide / dimethyl sulfoxide

5: hydroxylamine hydrochloride; sodium acetate / ethanol; water / Reflux

With hydrogenchloride; copper(l) iodide; n-butyllithium; hydroxylamine hydrochloride; water; sodium acetate; potassium carbonate; L-proline; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl acetamide; water; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2013.06.017

Reference yield:

: 1354812-21-7
(R)-3-(4-bromophenyl)-1-(6-methoxypyridin-3-yl)-3-o-tolylpropan-1-one

: 1354817-70-1
C₂₃H₂₄N₂O₄S

: 1354817-71-2
C₂₃H₂₄N₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; water / 1,4-dioxane / 1.5 h / 100 °C

2: potassium carbonate / N,N-dimethyl acetamide

3: L-proline; copper(l) iodide; sodium hydroxide / dimethyl sulfoxide

4: hydroxylamine hydrochloride; sodium acetate / ethanol; water / Reflux

With hydrogenchloride; copper(l) iodide; hydroxylamine hydrochloride; water; sodium acetate; potassium carbonate; L-proline; sodium hydroxide; In 1,4-dioxane; ethanol; N,N-dimethyl acetamide; water; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2013.06.017