[Pd(κ2-C,N-C(CO2Me)=C(CO2Me)C6H4(N=PPh3)-2)(N,N,N',N'-tetramethylethylenediamine)]ClO4*CDCl3

Base Information

• Chemical Name: [Pd(κ2-C,N-C(CO2Me)=C(CO2Me)C6H4(N=PPh3)-2)(N,N,N',N'-tetramethylethylenediamine)]ClO4*CDCl3
• CAS No.: 618912-17-7
• Molecular Formula: CHCl₃*C₃₆H₄₁N₃O₄PPd*ClO₄
• Molecular Weight: 936.954
• Mol file: 618912-17-7.mol

Synonyms:

Chemical Property of [Pd(κ2-C,N-C(CO2Me)=C(CO2Me)C6H4(N=PPh3)-2)(N,N,N',N'-tetramethylethylenediamine)]ClO4*CDCl3

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Pd(κ2-C,N-C(CO2Me)=C(CO2Me)C6H4(N=PPh3)-2)(N,N,N',N'-tetramethylethylenediamine)]ClO4*CDCl3

There total 4 articles about [Pd(κ2-C,N-C(CO2Me)=C(CO2Me)C6H4(N=PPh3)-2)(N,N,N',N'-tetramethylethylenediamine)]ClO4*CDCl3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-iodophenylimino)triphenylphosphorane (77116-72-4) → [Pd(κ2-C,N-C(CO2Me)=C(CO2Me)C6H4(N=PPh3)-2)(N,N,N',N'-tetramethylethylenediamine)]ClO4*CDCl3 (618912-17-7)

Guidance literature:

Multi-step reaction with 3 steps

1: toluene

2: acetone

3: diethyl ether; chloroform-d1

In diethyl ether; chloroform-d1; acetone; toluene;

DOI:10.1021/om0303552

Reference yield:

N,N,N,N,-tetramethylethylenediamine (110-18-9) → [Pd(κ2-C,N-C(CO2Me)=C(CO2Me)C6H4(N=PPh3)-2)(N,N,N',N'-tetramethylethylenediamine)]ClO4*CDCl3 (618912-17-7)

Guidance literature:

Multi-step reaction with 3 steps

1: toluene

2: acetone

3: diethyl ether; chloroform-d1

In diethyl ether; chloroform-d1; acetone; toluene;

DOI:10.1021/om0303552

Reference yield:

chloroform-d1 (865-49-6) + [Pd(κ2-C,N-C(CO2Me)=C(CO2Me)C6H4(N=PPh3)-2)(N,N,N',N'-tetramethylethylenediamine)]ClO4 (485844-31-3) → [Pd(κ2-C,N-C(CO2Me)=C(CO2Me)C6H4(N=PPh3)-2)(N,N,N',N'-tetramethylethylenediamine)]ClO4*CDCl3 (618912-17-7)

Guidance literature:

In diethyl ether; chloroform-d1;

DOI:10.1021/om0303552

upstream raw materials:

chloroform-d1

[Pd(κ2-C,N-C(CO2Me)=C(CO2Me)C6H4(N=PPh3)-2)(N,N,N',N'-tetramethylethylenediamine)]ClO4

(2-iodophenylimino)triphenylphosphorane

[Pd(C₆H₄(N=PPh₃)-2)I(N,N,N',N'-tetramethylethylenediamine)]