hexamethylbenzene-trishydrido-triphenylphosphine-ruthenium(IV)-hexafluorophosphate

Base Information

Chemical Name:hexamethylbenzene-trishydrido-triphenylphosphine-ruthenium(IV)-hexafluorophosphate
CAS No.:85413-06-5
Molecular Formula:C₃₀H₃₆PRu*F₆P
Molecular Weight:673.624
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Chemical Property of hexamethylbenzene-trishydrido-triphenylphosphine-ruthenium(IV)-hexafluorophosphate

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Technology Process of hexamethylbenzene-trishydrido-triphenylphosphine-ruthenium(IV)-hexafluorophosphate

There total 1 articles about hexamethylbenzene-trishydrido-triphenylphosphine-ruthenium(IV)-hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: ammonium hexafluorophosphate

: 82498-42-8
hexamethylbenzene-dihydrido-triphenylphosphine-ruthenium(II)

: 76-05-1
trifluoroacetic acid

: 85413-06-5
hexamethylbenzene-trishydrido-triphenylphosphine-ruthenium(IV)-hexafluorophosphate

Guidance literature:: In tetrahydrofuran; under Ar, Ru complex and NH4PF6 in THF soln. cooled to -78°C, added dropwise with stirring small excess of CF3COOH, stirred some min; decanted soln., washed with THF (3 portions) and once with methanol/ether (1/2), dried in vac., elem. anal.;
DOI:10.1016/S0022-328X(00)98565-6