Benzyloxycarbonylamino-thioacetic acid S-[(2R,3R)-3-(2-benzyloxycarbonylamino-acetylsulfanylmethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethyl] ester

Base Information

Chemical Name:Benzyloxycarbonylamino-thioacetic acid S-[(2R,3R)-3-(2-benzyloxycarbonylamino-acetylsulfanylmethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethyl] ester
CAS No.:125372-62-5
Molecular Formula:C₃₄H₄₆N₂O₁₂S₂
Molecular Weight:738.877
Hs Code.:

Benzyloxycarbonylamino-thioacetic acid S-[(2R,3R)-3-(2-benzyloxycarbonylamino-acetylsulfanylmethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethyl] ester

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Chemical Property of Benzyloxycarbonylamino-thioacetic acid S-[(2R,3R)-3-(2-benzyloxycarbonylamino-acetylsulfanylmethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethyl] ester

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Technology Process of Benzyloxycarbonylamino-thioacetic acid S-[(2R,3R)-3-(2-benzyloxycarbonylamino-acetylsulfanylmethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethyl] ester

There total 2 articles about Benzyloxycarbonylamino-thioacetic acid S-[(2R,3R)-3-(2-benzyloxycarbonylamino-acetylsulfanylmethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67654-51-7
(-)-(2R,3R)-2,3-bis(mercaptomethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 118385-04-9
Benzyloxycarbonylamino-thioacetic acid S-((2R,3R)-3-mercaptomethyl-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethyl) ester

: 125372-62-5
Benzyloxycarbonylamino-thioacetic acid S-[(2R,3R)-3-(2-benzyloxycarbonylamino-acetylsulfanylmethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethyl] ester

Guidance literature:: With triethylamine; diethyl dicarbonate; In N,N-dimethyl-formamide; 0 deg C, 1 h, then room t., 1 h;
DOI:10.1248/cpb.37.912

Reference yield:

: 67654-51-7
(-)-(2R,3R)-2,3-bis(mercaptomethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

: 5673-65-4
L-alanine p-nitrophenyl ester hydrobromide

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 125372-62-5
Benzyloxycarbonylamino-thioacetic acid S-[(2R,3R)-3-(2-benzyloxycarbonylamino-acetylsulfanylmethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethyl] ester

: 125412-50-2
(2S,3S)-S-(N-carbobenzyloxyglycyl)-S'-L-alanyl-2,3-bis(mercaptomethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane hydrochloride

Guidance literature:: With pyridine; triethylamine; diethyl dicarbonate; Yield given. Multistep reaction. Yields of byproduct given; 1.) DMF, 0 deg C, 1 h, then room t., 1 h, 2.) acetone, room t., 20 min;
DOI:10.1248/cpb.37.912