Technology Process of C27H35N3O6
There total 10 articles about C27H35N3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: trichlorophosphate / N,N-dimethyl-formamide
2: ammonium acetate
3: lithium aluminium tetrahydride
4: dmap
5: tetrakis(triphenylphosphine) palladium(0); copper(l) chloride; lithium chloride
6: ammonium acetate; palladium
7: salcomine; oxygen
With
dmap; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium(0); salcomine; ammonium acetate; oxygen; palladium; copper(l) chloride; lithium chloride; trichlorophosphate;
In
N,N-dimethyl-formamide;
2: Henry reaction;
DOI:10.1002/chem.201103605
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: sodium hydroxide / water
1.3: 215 °C
2.1: trichlorophosphate / N,N-dimethyl-formamide
3.1: ammonium acetate
4.1: lithium aluminium tetrahydride
5.1: dmap
6.1: tetrakis(triphenylphosphine) palladium(0); copper(l) chloride; lithium chloride
7.1: ammonium acetate; palladium
8.1: salcomine; oxygen
With
dmap; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium(0); salcomine; ammonium acetate; oxygen; palladium; copper(l) chloride; lithium chloride; sodium hydroxide; trichlorophosphate;
In
water; N,N-dimethyl-formamide;
3.1: Henry reaction;
DOI:10.1002/chem.201103605
- Guidance literature:
-
Multi-step reaction with 10 steps
1.1: potassium carbonate
2.1: sodium methylate / methanol
2.2: 160 °C
3.1: sodium hydroxide / water
3.3: 215 °C
4.1: trichlorophosphate / N,N-dimethyl-formamide
5.1: ammonium acetate
6.1: lithium aluminium tetrahydride
7.1: dmap
8.1: tetrakis(triphenylphosphine) palladium(0); copper(l) chloride; lithium chloride
9.1: ammonium acetate; palladium
10.1: salcomine; oxygen
With
dmap; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium(0); salcomine; ammonium acetate; oxygen; sodium methylate; potassium carbonate; palladium; copper(l) chloride; lithium chloride; sodium hydroxide; trichlorophosphate;
In
methanol; water; N,N-dimethyl-formamide;
2.1: Hemetsberger indole cyclization / 5.1: Henry reaction;
DOI:10.1002/chem.201103605