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Technology Process of (1S,8S,9S,RS)-11-benzyl-9-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>-6,11-diaza-7-oxatricyclo<4.3.1>dodecan-10,12-dione

(1S,8S,9S,RS)-11-benzyl-9-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>-6,11-diaza-7-oxatricyclo<4.3.1>dodecan-10,12-dione

Base Information
  • Chemical Name:(1S,8S,9S,RS)-11-benzyl-9-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>-6,11-diaza-7-oxatricyclo<4.3.1>dodecan-10,12-dione
  • CAS No.:139730-39-5
  • Molecular Formula:C26H34N2O5S
  • Molecular Weight:486.632
  • Hs Code.:
(1S,8S,9S,R<sub>S</sub>)-11-benzyl-9-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>-6,11-diaza-7-oxatricyclo<4.3.1>dodecan-10,12-dione

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Chemical Property of (1S,8S,9S,RS)-11-benzyl-9-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>-6,11-diaza-7-oxatricyclo<4.3.1>dodecan-10,12-dione
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Technology Process of (1S,8S,9S,RS)-11-benzyl-9-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>-6,11-diaza-7-oxatricyclo<4.3.1>dodecan-10,12-dione

There total 1 articles about (1S,8S,9S,RS)-11-benzyl-9-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>-6,11-diaza-7-oxatricyclo<4.3.1>dodecan-10,12-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 1.0%

2,3,4,5-tetrahydropyridine N-oxide
34418-91-2

2,3,4,5-tetrahydropyridine N-oxide

(R<sub>S</sub>)-N-benzyl-3-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>maleimide
132345-13-2

(RS)-N-benzyl-3-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>maleimide

(1S,8S,9S,R<sub>S</sub>)-11-benzyl-9-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>-6,11-diaza-7-oxatricyclo<4.3.1>dodecan-10,12-dione
139730-39-5

(1S,8S,9S,RS)-11-benzyl-9-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>-6,11-diaza-7-oxatricyclo<4.3.1>dodecan-10,12-dione

(R<sub>S</sub>)-11-benzyl-8-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>-6,11-diaza-7-oxatricyclo<4.3.1>dodecan-10,12-dione
139730-40-8

(RS)-11-benzyl-8-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>-6,11-diaza-7-oxatricyclo<4.3.1>dodecan-10,12-dione

Guidance literature:
In dichloromethane; at -78 ℃;
DOI:10.1016/S0957-4166(00)80034-8
upstream raw materials:

2,3,4,5-tetrahydropyridine N-oxide

(RS)-N-benzyl-3-<<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylsulphinyl>maleimide

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