F₂Si(O-C₆H₃-p-Me-o-N=N-C₆H₅)2

Base Information

Chemical Name:F₂Si(O-C₆H₃-p-Me-o-N=N-C₆H₅)2
CAS No.:1064021-43-7
Molecular Formula:C₂₆H₂₂F₂N₄O₂Si
Molecular Weight:488.569
Hs Code.:

F<sub>2</sub>Si(O-C<sub>6</sub>H<sub>3</sub>-p-Me-o-N=N-C<sub>6</sub>H<sub>5</sub>)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of F₂Si(O-C₆H₃-p-Me-o-N=N-C₆H₅)2

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Technology Process of F₂Si(O-C₆H₃-p-Me-o-N=N-C₆H₅)2

There total 1 articles about F₂Si(O-C₆H₃-p-Me-o-N=N-C₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1064021-40-4
Si(O-C₆H₃-p-Me-o-N=N-C₆H₅)4

: 109-63-7
trifluoroborane diethyl ether

: 1065010-70-9
F₂B(O-C₆H₃-p-Me-o-N=N-C₆H₅)

: 1064021-43-7
F₂Si(O-C₆H₃-p-Me-o-N=N-C₆H₅)2

Guidance literature:: In tetrahydrofuran; (Ar); a soln. of BF3*Et2O in dry THF added dropwise to soln. Si(O-C6H3-p-Me-o-N=N-C6H5)4 in the same solvent; after 14 days storage at ambient temp, F2(Si(O-C6H3-p-Me-o-N=N-C6H5)2 detected as main product and the boron compound as byproduct; solvent removed under vacuum; residue dissolved in toluene; hexane added; red crystals of the boron compound formed; filtered; dried in vacuum; elem. anal.;
DOI:10.1016/j.inoche.2007.05.005