3,3-dibenzyl-4-[5,5-dibenzyl-7-methyl-6-oxo-4-(triphenyl-λ⁵-phosphanylideneamino)-6,7-dihydro-5H-pyrrolo[3,2-e][1,3]oxazin-2-ylidene]-1-methyl-pyrrolidine-2,5-dione

Base Information

• Chemical Name: 3,3-dibenzyl-4-[5,5-dibenzyl-7-methyl-6-oxo-4-(triphenyl-λ⁵-phosphanylideneamino)-6,7-dihydro-5H-pyrrolo[3,2-e][1,3]oxazin-2-ylidene]-1-methyl-pyrrolidine-2,5-dione
• CAS No.: 55986-31-7
• Molecular Formula: C₅₈H₄₉N₄O₄P
• Molecular Weight: 897.025

Synonyms:

Chemical Property of 3,3-dibenzyl-4-[5,5-dibenzyl-7-methyl-6-oxo-4-(triphenyl-λ⁵-phosphanylideneamino)-6,7-dihydro-5H-pyrrolo[3,2-e][1,3]oxazin-2-ylidene]-1-methyl-pyrrolidine-2,5-dione

Chemical Property:

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Useful:

Technology Process of 3,3-dibenzyl-4-[5,5-dibenzyl-7-methyl-6-oxo-4-(triphenyl-λ⁵-phosphanylideneamino)-6,7-dihydro-5H-pyrrolo[3,2-e][1,3]oxazin-2-ylidene]-1-methyl-pyrrolidine-2,5-dione

There total 2 articles about 3,3-dibenzyl-4-[5,5-dibenzyl-7-methyl-6-oxo-4-(triphenyl-λ⁵-phosphanylideneamino)-6,7-dihydro-5H-pyrrolo[3,2-e][1,3]oxazin-2-ylidene]-1-methyl-pyrrolidine-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4-dibenzyl-1-methyl-2,5-dioxo-pyrrolidine-3-carbonitrile (42940-50-1) + dibromotriphenylphosphorane (1034-39-5) → 3,3-dibenzyl-4-[5,5-dibenzyl-7-methyl-6-oxo-4-(triphenyl-λ5-phosphanylideneamino)-6,7-dihydro-5H-pyrrolo[3,2-e][1,3]oxazin-2-ylidene]-1-methyl-pyrrolidine-2,5-dione (55986-31-7,57519-73-0)

Guidance literature:

With triethylamine; In benzene; Heating;

Reference yield:

4,4-dibenzyl-3-bromo-1-methyl-2,5-dioxo-pyrrolidine-3-carbonitrile (35789-65-2) + triphenylphosphine (603-35-0) → 3,3-dibenzyl-4-[5,5-dibenzyl-7-methyl-6-oxo-4-(triphenyl-λ5-phosphanylideneamino)-6,7-dihydro-5H-pyrrolo[3,2-e][1,3]oxazin-2-ylidene]-1-methyl-pyrrolidine-2,5-dione (55986-31-7,57519-73-0)

Guidance literature:

In benzene; for 72h; Heating;

DOI:10.1016/S0040-4020(01)97403-4

upstream raw materials:

4,4-dibenzyl-1-methyl-2,5-dioxo-pyrrolidine-3-carbonitrile

dibromotriphenylphosphorane

4,4-dibenzyl-3-bromo-1-methyl-2,5-dioxo-pyrrolidine-3-carbonitrile

triphenylphosphine

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