Technology Process of C14H11NO3
There total 6 articles about C14H11NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride / ethanol / 6 h / Heating
2: tetrahydrofuran / 12 h
With
hydroxylamine hydrochloride;
In
tetrahydrofuran; ethanol;
DOI:10.3987/COM-11-12162
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetrahydrofuran; methanol
2.1: n-butyllithium / Norlaudanosolin / -13 - -10 °C
2.3: Acidic aq. solution
3.1: potassium hydroxide / water; dimethyl sulfoxide / 9 h / Reflux
4.1: hydroxylamine hydrochloride / ethanol / 6 h / Heating
5.1: tetrahydrofuran / 12 h
With
n-butyllithium; hydroxylamine hydrochloride; potassium hydroxide;
In
tetrahydrofuran; methanol; ethanol; Norlaudanosolin; water; dimethyl sulfoxide;
DOI:10.3987/COM-11-12162
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: thionyl chloride / N,N-dimethyl-formamide / Heating
2.1: tetrahydrofuran; methanol
3.1: n-butyllithium / Norlaudanosolin / -13 - -10 °C
3.3: Acidic aq. solution
4.1: potassium hydroxide / water; dimethyl sulfoxide / 9 h / Reflux
5.1: hydroxylamine hydrochloride / ethanol / 6 h / Heating
6.1: tetrahydrofuran / 12 h
With
n-butyllithium; thionyl chloride; hydroxylamine hydrochloride; potassium hydroxide;
In
tetrahydrofuran; methanol; ethanol; Norlaudanosolin; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.3987/COM-11-12162