4,4-dimethyl-3-triphenylsilyl-5,5-bis(trimethylsilyl)-1,2,3-triaza-4-germa-1-cyclopentene

Base Information

Chemical Name:4,4-dimethyl-3-triphenylsilyl-5,5-bis(trimethylsilyl)-1,2,3-triaza-4-germa-1-cyclopentene
CAS No.:108148-65-8
Molecular Formula:C₂₇H₃₉GeN₃Si₃
Molecular Weight:562.473
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4-dimethyl-3-triphenylsilyl-5,5-bis(trimethylsilyl)-1,2,3-triaza-4-germa-1-cyclopentene

Chemical Property:

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Technology Process of 4,4-dimethyl-3-triphenylsilyl-5,5-bis(trimethylsilyl)-1,2,3-triaza-4-germa-1-cyclopentene

There total 1 articles about 4,4-dimethyl-3-triphenylsilyl-5,5-bis(trimethylsilyl)-1,2,3-triaza-4-germa-1-cyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103349-20-8
Ge(CH₃)2BrCBr[Si(CH₃)3]2

: 5599-34-8
triphenylsilyl azide

: 108148-65-8
4,4-dimethyl-3-triphenylsilyl-5,5-bis(trimethylsilyl)-1,2,3-triaza-4-germa-1-cyclopentene

Guidance literature:: With n-butyllithium; In diethyl ether; byproducts: LiBr, n-C4H9Br; dropwise addn. of n-BuLi in Et2O or hexane to a mixt. of the dibromide and the azide in Et2O at -78°C; under exclusion of water and air; removal of the solvent at room temp. under high vacuum; addn. of pentane at -78°C; decantation or filtration at -78°C; concn.; crystn. at -78°C; elem. anal.;

Reference yield:

: 108148-65-8
4,4-dimethyl-3-triphenylsilyl-5,5-bis(trimethylsilyl)-1,2,3-triaza-4-germa-1-cyclopentene

: 108149-04-8
1,3-bis(dimethylphenylgermyl)-2,2,4,4-tetraphenyl-1,3-diaza-2,4-disilacyclobutane

Guidance literature:: In diethyl ether; byproducts: ((CH3)3Si)2CN2; thermolysis in Et2O at 5°C for 3 h under exclusion of water and air;

Reference yield:

: 108148-65-8
4,4-dimethyl-3-triphenylsilyl-5,5-bis(trimethylsilyl)-1,2,3-triaza-4-germa-1-cyclopentene

: 108148-92-1
2,2,4,4-tetramethyl-1,3-bis(triphenylsilyl)-1,3-diaza-2,4-digermacyclobutane

Guidance literature:: In pentane; byproducts: ((CH3)3Si)2CN2; thermolysis in pentane at 25°C for 3 h under exclusion of water and air; elem. anal.;