HRe(P(C₆H₅)3)((CH₃)2PCH₂CH₂P(CH₃)2)2

Base Information

Chemical Name:HRe(P(C₆H₅)3)((CH₃)2PCH₂CH₂P(CH₃)2)2
CAS No.:108453-42-5
Molecular Formula:C₃₀H₄₈P₅Re
Molecular Weight:749.787
Hs Code.:

HRe(P(C<sub>6</sub>H<sub>5</sub>)3)((CH<sub>3</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(CH<sub>3</sub>)2)2

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Chemical Property of HRe(P(C₆H₅)3)((CH₃)2PCH₂CH₂P(CH₃)2)2

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Technology Process of HRe(P(C₆H₅)3)((CH₃)2PCH₂CH₂P(CH₃)2)2

There total 2 articles about HRe(P(C₆H₅)3)((CH₃)2PCH₂CH₂P(CH₃)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: HRe(P(C₆H₅)3)((CH₃)2PCH₂CH₂P(CH₃)2)2

: 108453-42-5
HRe(P(C₆H₅)3)((CH₃)2PCH₂CH₂P(CH₃)2)2

Guidance literature:: In tetrahydrofuran-d8; isomerization in THF-d8 at 27°C; not isolated, monitored by 1H-NMR (ratio 1:1.44);

Reference yield:

: 81368-84-5
(C₅H₆)Re(P(C₆H₅)3)2H₃

: 23936-60-9
1,2-bis(dimethylphosphanyl)ethane

: HRe(P(C₆H₅)3)((CH₃)2PCH₂CH₂P(CH₃)2)2

: 108453-42-5
HRe(P(C₆H₅)3)((CH₃)2PCH₂CH₂P(CH₃)2)2

Guidance literature:: In benzene-d6; benzene; a complex and 5 equiv. of ligand were placed under vacuum in a NMR tube, then solvents were vacuum transferred into the tube which was 3 times freeze-pump-thaw degassed and heated at 50°C for 2 weeks; cis-isomer pptd. on slow evapn. of solvent; purified by recrystallization from THF-hexane; elem. anal.;