1,6-Hexanedione, 1,6-diphenyl-, dihydrazone

Base Information

Chemical Name:1,6-Hexanedione, 1,6-diphenyl-, dihydrazone
CAS No.:140903-04-4
Molecular Formula:C₁₈H₂₂N₄
Molecular Weight:294.399
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-Hexanedione, 1,6-diphenyl-, dihydrazone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,6-Hexanedione, 1,6-diphenyl-, dihydrazone

There total 1 articles about 1,6-Hexanedione, 1,6-diphenyl-, dihydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3375-38-0
1,4-dibenzoylbutane

: 140903-04-4
1,6-Diphenyl-1,6-hexanedione dihydrazone

Guidance literature:: With hydrazine hydrate; In ethanol; for 12h; Heating;
DOI:10.1021/jo00037a021

Reference yield:

: 140903-04-4
1,6-Diphenyl-1,6-hexanedione dihydrazone

: 21266-01-3
1,6-Bis(diazo)-1,6-diphenylhexane

Guidance literature:: With potassium hydroxide; sodium sulfate; mercury(II) oxide; In diethyl ether; for 6h; Yield given; Ambient temperature;
DOI:10.1021/jo00037a021

Reference yield:

: 140903-04-4
1,6-Diphenyl-1,6-hexanedione dihydrazone

: 41317-87-7
1,2-diphenylcyclohex-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: yellow mercuric oxide, Na₂SO₄, sat. KOH-EtOH / diethyl ether / 6 h / Ambient temperature

2: 96 percent Chromat_. / 9,10-dicyanoanthracene (DCA) / acetonitrile / 0.08 h / Irradiation; also with Cu(II)-perchlorate

With potassium hydroxide; 9,10-Dicyanoanthracene; sodium sulfate; mercury(II) oxide; In diethyl ether; acetonitrile;
DOI:10.1021/jo00037a021