[PdCl([(η5-C5H4)-CHO]Fe[(η5-C5H3)-CH=N(cyclohexyl)])(tricyclohexylphosphine)]

Base Information

• Chemical Name: [PdCl([(η5-C5H4)-CHO]Fe[(η5-C5H3)-CH=N(cyclohexyl)])(tricyclohexylphosphine)]
• CAS No.: 915790-09-9
• Molecular Formula: C₃₆H₅₃ClFeNOPPd
• Molecular Weight: 744.517
• Mol file: 915790-09-9.mol

Synonyms:

Chemical Property of [PdCl([(η5-C5H4)-CHO]Fe[(η5-C5H3)-CH=N(cyclohexyl)])(tricyclohexylphosphine)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [PdCl([(η5-C5H4)-CHO]Fe[(η5-C5H3)-CH=N(cyclohexyl)])(tricyclohexylphosphine)]

There total 1 articles about [PdCl([(η5-C5H4)-CHO]Fe[(η5-C5H3)-CH=N(cyclohexyl)])(tricyclohexylphosphine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

lithium tetrachloropalladate + cyclohexyl 1,1'-bisferrocenylimine (916906-88-2) + tricyclohexylphosphine (2622-14-2) → [PdCl([(η5-C5H4)-CHO]Fe[(η5-C5H3)-CH=N(cyclohexyl)])(tricyclohexylphosphine)] (915790-09-9)

Guidance literature:

With NaOAc; In methanol; dichloromethane; Fe-compound reacted with two mole equiv. of Li2PdCl4 and NaOAc in CH3OH at room temp. for 24 h; collected by filtration; washed several times with CH3OH; treated with two equiv. of PCy3 in dry CH2Cl2 at room temp. for 0.5 h; sepd. by passing through short silica gel column with CH2Cl2 as eluent; solvent evapd.; elem. anal.;

DOI:10.1016/j.inoche.2006.02.008

upstream raw materials:

cyclohexyl 1,1'-bisferrocenylimine

tricyclohexylphosphine