cyclohexyl 1,1'-bisferrocenylimine

Base Information

Chemical Name:cyclohexyl 1,1'-bisferrocenylimine
CAS No.:916906-88-2
Molecular Formula:C₂₄H₃₂FeN₂
Molecular Weight:404.378
Hs Code.:

Synonyms:cyclohexyl 1,1'-bisferrocenylimine

Suppliers and Price of cyclohexyl 1,1'-bisferrocenylimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of cyclohexyl 1,1'-bisferrocenylimine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of cyclohexyl 1,1'-bisferrocenylimine

There total 1 articles about cyclohexyl 1,1'-bisferrocenylimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1271-48-3
1,1'-ferrocenyldicarboxaldehyde

: 108-91-8,157973-60-9
cyclohexylamine

: 916906-88-2
cyclohexyl 1,1'-bisferrocenylimine

Guidance literature:: With activated Al₂O₃; In toluene; (N2); cyclohexylamine added to soln. of Fe-compound in dry toluene; refluxed with stirring in the presence of freshly activated Al2O3 for ca. 3 h; filtrated; solvents evapd.; recrystallized from CH2Cl2/petroleum ether; elem. anal.;
DOI:10.1016/j.inoche.2006.02.008

Reference yield:

: lithium tetrachloropalladate

: 916906-88-2
cyclohexyl 1,1'-bisferrocenylimine

: 2622-14-2
tricyclohexylphosphine

: 915790-09-9
[PdCl([(η5-C5H4)-CHO]Fe[(η5-C5H3)-CH=N(cyclohexyl)])(tricyclohexylphosphine)]

Guidance literature:: With NaOAc; In methanol; dichloromethane; Fe-compound reacted with two mole equiv. of Li2PdCl4 and NaOAc in CH3OH at room temp. for 24 h; collected by filtration; washed several times with CH3OH; treated with two equiv. of PCy3 in dry CH2Cl2 at room temp. for 0.5 h; sepd. by passing through short silica gel column with CH2Cl2 as eluent; solvent evapd.; elem. anal.;
DOI:10.1016/j.inoche.2006.02.008