2,2,4,4-tetra(2,4,6-tri-isopropylphenyl)-1,3-dithia-2,4-stannetane

Base Information

Chemical Name:2,2,4,4-tetra(2,4,6-tri-isopropylphenyl)-1,3-dithia-2,4-stannetane
CAS No.:126857-71-4
Molecular Formula:C₆₀H₉₂S₂Sn₂
Molecular Weight:1114.94
Hs Code.:

Synonyms:

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Chemical Property of 2,2,4,4-tetra(2,4,6-tri-isopropylphenyl)-1,3-dithia-2,4-stannetane

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Technology Process of 2,2,4,4-tetra(2,4,6-tri-isopropylphenyl)-1,3-dithia-2,4-stannetane

There total 8 articles about 2,2,4,4-tetra(2,4,6-tri-isopropylphenyl)-1,3-dithia-2,4-stannetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 10544-50-0
sulfur

: 98526-67-1
hexakis(2,4,6-tri-isopropylphenyl) cyclotristannane

: 134391-62-1
(2,4,6-triisopropylbenzene)4(1,2-dithiadistannetane)

: 126857-71-4
2,2,4,4-tetra(2,4,6-tri-isopropylphenyl)-1,3-dithia-2,4-stannetane

: 126857-72-5
((2,4,6-iPr₃C₆H₂)2Sn)2S

Guidance literature:: In toluene; S8 added to the Sn-compd. in toluene at 90°C, standing at 90°C, 0.5h, colour change from red to yellow; toluene replaced by pentane, filtered, crystn.;

Reference yield: 27.0%

: sodiumsulfide nonahydrate

: 124593-69-7
1,1,2,2-tetra(2,4,6-tri-isopropylphenyl)-1,2-dibromoditin

: 126857-71-4
2,2,4,4-tetra(2,4,6-tri-isopropylphenyl)-1,3-dithia-2,4-stannetane

: 126857-70-3
2,2,4,4-tetra(2,4,6-tri-isopropylphenyl)-1-oxa-3-thia-2,4-stannetane

Guidance literature:: In ethanol; water; toluene; aq. soln. of Na2S was added to soln. of Sn compd. in EtOH/toluene (2:1) and refluxed for 48 h, after removal of solvent residue was partitioned between toluene/water; product yielded from organic layer; recrystn. from EtOH/hexane; elem. anal.;
DOI:10.1039/c39890001621