Technology Process of C2HF3O2*C23H29ClN6O5
There total 4 articles about C2HF3O2*C23H29ClN6O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 0.08 h / 20 °C
1.2: 15 h / 100 °C
1.3: 3 h / 20 - 30 °C
2.1: magnesium sulfate / N,N-dimethyl acetamide; acetonitrile / 80 °C
3.1: dichloromethane / 15 h / 20 °C
With
magnesium sulfate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; N,N-dimethyl acetamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic acid; zinc / 0 - 20 °C
2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 0.08 h / 20 °C
2.2: 15 h / 100 °C
2.3: 3 h / 20 - 30 °C
3.1: magnesium sulfate / N,N-dimethyl acetamide; acetonitrile / 80 °C
4.1: dichloromethane / 15 h / 20 °C
With
magnesium sulfate; acetic acid; N-ethyl-N,N-diisopropylamine; zinc;
In
dichloromethane; N,N-dimethyl acetamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridinium hydrobromide perbromide / tert-butyl alcohol / 20 °C
2.1: acetic acid; zinc / 0 - 20 °C
3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 0.08 h / 20 °C
3.2: 15 h / 100 °C
3.3: 3 h / 20 - 30 °C
4.1: magnesium sulfate / N,N-dimethyl acetamide; acetonitrile / 80 °C
5.1: dichloromethane / 15 h / 20 °C
With
pyridinium hydrobromide perbromide; magnesium sulfate; acetic acid; N-ethyl-N,N-diisopropylamine; zinc;
In
dichloromethane; N,N-dimethyl acetamide; acetonitrile; tert-butyl alcohol;