[(o-diphenylphosphinoferrocene sulfonate)Pd(methyl)(pyridine)]

Base Information

• Chemical Name: [(o-diphenylphosphinoferrocene sulfonate)Pd(methyl)(pyridine)]
• CAS No.: 1334528-45-8
• Molecular Formula: C₂₈H₂₆FeNO₃PPdS
• Molecular Weight: 649.826
• Mol file: 1334528-45-8.mol

Synonyms:

Chemical Property of [(o-diphenylphosphinoferrocene sulfonate)Pd(methyl)(pyridine)]

Chemical Property:

Purity/Quality:

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Technology Process of [(o-diphenylphosphinoferrocene sulfonate)Pd(methyl)(pyridine)]

There total 1 articles about [(o-diphenylphosphinoferrocene sulfonate)Pd(methyl)(pyridine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

pyridine (110-86-1) + (N,N,N',N'-tetramethylethylenediamine)dimethylpalladium(II) + o-diphenylphosphinoferrocene sulfonic acid (1334528-39-0) → [(o-diphenylphosphinoferrocene sulfonate)Pd(methyl)(pyridine)] (1334528-45-8)

Guidance literature:

In tetrahydrofuran; (Ar), Schlenk techniques; addn. of THF to Fe complex, addn. of Pd complex at 0°C, stirring overnight, addn. of Py; filtration afer 2 h, washing (CH2Cl2), pptn. by ether, filtration, storage at -32°C for 2 d, filtration, elem. anal.;

DOI:10.1021/om200628r

upstream raw materials:

pyridine

o-diphenylphosphinoferrocene sulfonic acid