Technology Process of C34H43FN3O6PSi
There total 1 articles about C34H43FN3O6PSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: ethanol / 2 h / 60 °C
2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 1.5 h / 0 °C
2.2: 1.5 h / 0 °C
With
N-Bromosuccinimide;
In
ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 25 °C
2.1: triethylamine / dichloromethane / 0.17 h / 0 - 25 °C
3.1: calcium carbonate; lithium iodide / acetonitrile / 1 h / 80 °C
4.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / 0 °C
4.2: 1.08 h / 0 °C
With
potassium tert-butylate; tetrabutyl ammonium fluoride; triethylamine; calcium carbonate; lithium iodide;
In
tetrahydrofuran; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 25 °C
2.1: triethylamine / dichloromethane / 0.17 h / 0 - 25 °C
3.1: calcium carbonate; lithium iodide / acetonitrile / 1 h / 80 °C
4.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / 0 °C
4.2: 1.08 h / 0 °C
5.1: Chiracel OD column / hexanes; isopropyl alcohol / Resolution of racemate
With
Chiracel OD column; potassium tert-butylate; tetrabutyl ammonium fluoride; triethylamine; calcium carbonate; lithium iodide;
In
tetrahydrofuran; hexanes; dichloromethane; isopropyl alcohol; acetonitrile;