((C₃H₇)3P)2OsCl₃NC₆H₁₀

Base Information

• Chemical Name: ((C₃H₇)3P)2OsCl₃NC₆H₁₀
• CAS No.: 288324-69-6
• Molecular Formula: C₂₄H₅₂Cl₃NOsP₂
• Molecular Weight: 713.19

Synonyms:

Chemical Property of ((C₃H₇)3P)2OsCl₃NC₆H₁₀

Chemical Property:

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Technology Process of ((C₃H₇)3P)2OsCl₃NC₆H₁₀

There total 1 articles about ((C₃H₇)3P)2OsCl₃NC₆H₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

cyclohexanone-oxime (100-64-1) + ((C3H7)3P)2OsH2Cl2 → ((C3H7)3P)2OsCl3NC6H10 (288324-69-6) + [OsHCl2(P(CH(CH3)2)3)2NC(CH2)4CH2] (288324-67-4) + OsH2Cl(κN,κO-[ON=C(CH2)4CH2])(P(i)Pr3)2 (249630-71-5)

Guidance literature:

In toluene; brown soln. of Os complex treated with imine under Ar; refluxed for 1 h; concd., MeOH added, yellow ppt. washed and dried in vacuo; purified by recrystallization from toluene-MeOH; identified by elem. anal., IR, NMR,mass spectra and single crystal X-ray diffraction;

DOI:10.1021/om000208t

upstream raw materials:

cyclohexanone-oxime

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