Technology Process of C33H37N3O6
There total 5 articles about C33H37N3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: oxalyl dichloride / 1,2-dichloro-ethane / 20 °C / Inert atmosphere; Cooling with ice
1.2: 0 - 20 °C / Inert atmosphere
2.1: aluminum (III) chloride / 1,2-dichloro-ethane / 20 °C / Inert atmosphere
3.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 100 °C
3.2: 15 h / Reflux
4.1: pyridine / methanol / 4 h / Reflux
With
pyridine; aluminum (III) chloride; oxalyl dichloride; potassium carbonate;
In
methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201200316
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen; palladium 10% on activated carbon / ethanol / 20 h / 20 °C / 760.05 Torr
2.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 100 °C
2.2: 15 h / Reflux
3.1: pyridine / methanol / 4 h / Reflux
With
pyridine; palladium 10% on activated carbon; hydrogen; potassium carbonate;
In
methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201200316
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: aluminum (III) chloride / 1,2-dichloro-ethane / 20 °C / Inert atmosphere
2.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 100 °C
2.2: 15 h / Reflux
3.1: pyridine / methanol / 4 h / Reflux
With
pyridine; aluminum (III) chloride; potassium carbonate;
In
methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201200316
