Technology Process of C19H26N2O3S
There total 3 articles about C19H26N2O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-oxocycloheptanecarbonitrile;
With
2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine;
In
tetrahydrofuran;
at 25 ℃;
for 0.166667h;
Inert atmosphere;
N-mesitylenesulfonyl aziridine;
In
tetrahydrofuran;
at 65 ℃;
for 6h;
Catalytic behavior;
Inert atmosphere;
DOI:10.1002/chem.201203825
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine / -10 - 20 °C / Inert atmosphere
2.1: potassium hydroxide / water; toluene / 25 °C / Inert atmosphere
3.1: 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine / tetrahydrofuran / 0.17 h / 25 °C / Inert atmosphere
3.2: 6 h / 65 °C / Inert atmosphere
With
pyridine; 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine; potassium hydroxide;
In
tetrahydrofuran; water; toluene;
DOI:10.1002/chem.201203825
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydroxide / water; toluene / 25 °C / Inert atmosphere
2.1: 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine / tetrahydrofuran / 0.17 h / 25 °C / Inert atmosphere
2.2: 6 h / 65 °C / Inert atmosphere
With
2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine; potassium hydroxide;
In
tetrahydrofuran; water; toluene;
DOI:10.1002/chem.201203825