imidazole-1-carboxylic acid cyclopentylphenylpropoxycarbonylmethyl ester

Base Information

Chemical Name:imidazole-1-carboxylic acid cyclopentylphenylpropoxycarbonylmethyl ester
CAS No.:1404453-83-3
Molecular Formula:C₂₀H₂₄N₂O₄
Molecular Weight:356.422
Hs Code.:

Synonyms:

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Chemical Property of imidazole-1-carboxylic acid cyclopentylphenylpropoxycarbonylmethyl ester

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Technology Process of imidazole-1-carboxylic acid cyclopentylphenylpropoxycarbonylmethyl ester

There total 3 articles about imidazole-1-carboxylic acid cyclopentylphenylpropoxycarbonylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15206-55-0
methyl 2-oxo-2-phenylacetate

: 1404453-82-2
cyclopentylhydroxyphenylacetic acid propyl ester

: 1404453-83-3
imidazole-1-carboxylic acid cyclopentylphenylpropoxycarbonylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine; magnesium / tetrahydrofuran / 0 °C / Reflux; Inert atmosphere

1.2: 10 - 20 °C / Inert atmosphere

2.1: sodium hydroxide / water; methanol / 20 °C / Inert atmosphere

3.1: N,N-dimethyl-formamide / 18 h / 70 °C / Inert atmosphere

3.2: 24 h / 70 °C / Inert atmosphere

With iodine; magnesium; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/op3001788

Reference yield:

: 19833-96-6
2-Cyclopentyl-2-hydroxy-2-phenylacetic acid methyl ester

: 1404453-82-2
cyclopentylhydroxyphenylacetic acid propyl ester

: 1404453-83-3
imidazole-1-carboxylic acid cyclopentylphenylpropoxycarbonylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / water; methanol / 20 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide / 18 h / 70 °C / Inert atmosphere

2.2: 24 h / 70 °C / Inert atmosphere

With sodium hydroxide; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/op3001788

Reference yield:

: 71-23-8
propan-1-ol

: 427-49-6
2-cyclopentyl-2-hydroxy-2-phenylacetic acid

: 530-62-1
1,1'-carbonyldiimidazole

: 1404453-82-2
cyclopentylhydroxyphenylacetic acid propyl ester

: 1404453-83-3
imidazole-1-carboxylic acid cyclopentylphenylpropoxycarbonylmethyl ester

Guidance literature:: 2-cyclopentyl-2-hydroxy-2-phenylacetic acid; 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 70 ℃; for 18h; Inert atmosphere;

propan-1-ol; In N,N-dimethyl-formamide; at 70 ℃; for 24h; Inert atmosphere;
DOI:10.1021/op3001788