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PdCl3P(C6H5)3(1-)*P(C6H5)3(CH2CH2COCH3)(1+)={PdCl3P(C6H5)3}{P(C6H5)3(CH2CH2COCH3)}

Base Information
  • Chemical Name:PdCl3P(C6H5)3(1-)*P(C6H5)3(CH2CH2COCH3)(1+)={PdCl3P(C6H5)3}{P(C6H5)3(CH2CH2COCH3)}
  • CAS No.:88325-31-9
  • Molecular Formula:C18H15Cl3PPd*C22H22OP
  • Molecular Weight:808.46
  • Hs Code.:
PdCl<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)3<sup>(1-)</sup>*P(C<sub>6</sub>H<sub>5</sub>)3(CH<sub>2</sub>CH<sub>2</sub>COCH<sub>3</sub>)<sup>(1+)</sup>={PdCl<sub>3</sub>P(C<sub>6</sub>H<sub>5</sub>)3}{P(C<sub>6</sub>H<sub>5</sub>)3(CH<sub>2</sub>CH<sub>2</sub>COCH<sub>3</sub>)}

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Chemical Property of PdCl3P(C6H5)3(1-)*P(C6H5)3(CH2CH2COCH3)(1+)={PdCl3P(C6H5)3}{P(C6H5)3(CH2CH2COCH3)}
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Technology Process of PdCl3P(C6H5)3(1-)*P(C6H5)3(CH2CH2COCH3)(1+)={PdCl3P(C6H5)3}{P(C6H5)3(CH2CH2COCH3)}

There total 3 articles about PdCl3P(C6H5)3(1-)*P(C6H5)3(CH2CH2COCH3)(1+)={PdCl3P(C6H5)3}{P(C6H5)3(CH2CH2COCH3)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogenchloride; carbon monoxide; In ethanol; React. between Pd-complex, CH3COCH2CH2Cl and EtOH soln. of HCl under 100 atm CO at 80°C for 2 h in an autoclave.; Cooling of autoclave to room temp., slow depressurizing after several hours, filtn. of suspn., washing of ppt. (ethyl ether), drying in vac. Identification of resulting cryst. by elem. and IR anal.;
DOI:10.1016/0304-5102(90)85045-J
Guidance literature:
In ethanol; Pd-complex was treated with excess of ligand in boiling EtOH for some h; cooled, allowed to stand, sepd. out;
DOI:10.1016/S0020-1693(00)91184-8
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