(1-benzyl-3a,4-7,7a-η6-indene)chromium tricarbonyl

Base Information

• Chemical Name: (1-benzyl-3a,4-7,7a-η6-indene)chromium tricarbonyl
• CAS No.: 82397-21-5
• Molecular Formula: C₁₉H₁₄CrO₃
• Molecular Weight: 342.314
• Mol file: 82397-21-5.mol

Synonyms:

Chemical Property of (1-benzyl-3a,4-7,7a-η6-indene)chromium tricarbonyl

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (1-benzyl-3a,4-7,7a-η6-indene)chromium tricarbonyl

There total 1 articles about (1-benzyl-3a,4-7,7a-η6-indene)chromium tricarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

potassium (η5-indenyl-tricarbonylchromium) + benzyl bromide (100-39-0) → (1-benzyl-3a,4-7,7a-η6-indene)chromium tricarbonyl (82397-21-5)

Guidance literature:

In tetrahydrofuran; org. compd. added at once to THF soln. of Cr complex under Ar, mixture stirred at 30-35°C for 15-20 min; evapn. in vac., extn. (hexane), concn., cooling to -70°C, filtration, chromy. (SiO2, benzene/petroleum ether), removal of solvent, recrystn. (benzene/heptane);

DOI:10.1016/S0022-328X(00)83408-7

upstream raw materials:

benzyl bromide