meso-tetra(p-tolyl)porphinatoiron(III) methoxide

Base Information

Chemical Name:meso-tetra(p-tolyl)porphinatoiron(III) methoxide
CAS No.:83951-56-8
Molecular Formula:C₄₉H₃₉FeN₄O
Molecular Weight:755.722
Hs Code.:

Synonyms:

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Chemical Property of meso-tetra(p-tolyl)porphinatoiron(III) methoxide

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Technology Process of meso-tetra(p-tolyl)porphinatoiron(III) methoxide

There total 1 articles about meso-tetra(p-tolyl)porphinatoiron(III) methoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19496-18-5
5,10,15,20-tetrakis(4-methylphenyl)porphyrinatoiron(III) chloride

: 124-41-4
sodium methylate

: 83951-56-8
meso-tetra(p-tolyl)porphinatoiron(III) methoxide

Guidance literature:: In methanol; dichloromethane; soln. of the sodium alkoxide added gradually to a CH2Cl2 soln. of TTPFeCl; filtered, evapd. (hot plate), crystals collected (glass frit), washed (hot methanol), dried (vac., room temp., 24 h);
DOI:10.1016/S0020-1693(00)80830-0

Reference yield:

: 83951-56-8
meso-tetra(p-tolyl)porphinatoiron(III) methoxide

: N-hydroxy-succinimide anion

: 122104-78-3
meso-tetra(p-tolyl)porphinatoiron(III) N-hydroxysuccinimide

Guidance literature:: In dichloromethane; acetone; acetone soln. of the N-hydroxyimide added to a CH2Cl2 soln. of TTPFeOCH3; evapd. (vac., low heat), residue stirred with benzene, excess N-hydroxyimide removed by filtration, evapd., hexane added slowly, crystn., dried (vac., room temp., 24 h);
DOI:10.1016/S0020-1693(00)80830-0

Reference yield:

: 83951-56-8
meso-tetra(p-tolyl)porphinatoiron(III) methoxide

: 40213-71-6
benzohydroxamate anion

: 122104-75-0
meso-tetra(p-tolyl)porphinatoiron(III) benzohydroxamate

Guidance literature:: In sulfuric acid; benzene; aq. H2SO4; soln. of the anion in dild. aq. sulfuric acid stirred with benzene contg. TTPFeOCH3 (10 min); benzene layer sepd., dried over anhydrous Na2SO4, vol. reduced, hexane added slowly, crystn., washed (ether), dried (vac., room temp., 24 h);
DOI:10.1016/S0020-1693(00)80830-0