C₂₂H₂₃NO₆

Base Information

• Chemical Name: C₂₂H₂₃NO₆
• CAS No.: 1314140-71-0
• Molecular Formula: C₂₂H₂₃NO₆
• Molecular Weight: 397.428
• Mol file: 1314140-71-0.mol

Synonyms:

Chemical Property of C₂₂H₂₃NO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₃NO₆

There total 4 articles about C₂₂H₂₃NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(4-methoxy-phenyl)-3-oxo-propionaldehyde (31706-15-7) → C22H23NO6 (1314140-71-0) + dimethyl 3-(4-methoxyphenyl)-5-[methyl(phenyl)amino]furan-2,2(5H)-dicarboxylate (1314140-56-1) + dimethyl 3-(4-methoxybenzoyl)-1-methylquinoline-4,4(1H)-dicarboxylate (1314140-57-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: thionyl chloride / benzene / Inert atmosphere

2.1: benzene / Reflux; Inert atmosphere

3.1: copper acetylacetonate / benzene / Reflux; Inert atmosphere

3.2: 2.5 h / Inert atmosphere

With copper acetylacetonate; thionyl chloride; In benzene;

DOI:10.1002/hlca.201000386

Reference yield:

1-(4-methoxyphenyl)ethanone (100-06-1) → C22H23NO6 (1314140-71-0) + dimethyl 3-(4-methoxyphenyl)-5-[methyl(phenyl)amino]furan-2,2(5H)-dicarboxylate (1314140-56-1) + dimethyl 3-(4-methoxybenzoyl)-1-methylquinoline-4,4(1H)-dicarboxylate (1314140-57-2)

Guidance literature:

Multi-step reaction with 4 steps

1.1: methanol; sodium hydride / diethyl ether / 0.67 h / 5 - 10 °C / Inert atmosphere

1.2: Cooling; Inert atmosphere

2.1: thionyl chloride / benzene / Inert atmosphere

3.1: benzene / Reflux; Inert atmosphere

4.1: copper acetylacetonate / benzene / Reflux; Inert atmosphere

4.2: 2.5 h / Inert atmosphere

With methanol; copper acetylacetonate; thionyl chloride; sodium hydride; In diethyl ether; benzene;

DOI:10.1002/hlca.201000386

Reference yield:

β-chlorovinyl(p-anisyl)ketone (15787-86-7) + N-methylaniline (100-61-8) → C22H23NO6 (1314140-71-0) + dimethyl 3-(4-methoxyphenyl)-5-[methyl(phenyl)amino]furan-2,2(5H)-dicarboxylate (1314140-56-1) + dimethyl 3-(4-methoxybenzoyl)-1-methylquinoline-4,4(1H)-dicarboxylate (1314140-57-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: benzene / Reflux; Inert atmosphere

2.1: copper acetylacetonate / benzene / Reflux; Inert atmosphere

2.2: 2.5 h / Inert atmosphere

With copper acetylacetonate; In benzene;

DOI:10.1002/hlca.201000386

upstream raw materials:

β-chlorovinyl(p-anisyl)ketone

N-methylaniline

dimethyl diazomalonate

(2E)-1-(4-methoxyphenyl)-3-[methyl(phenyl)amino]prop-2-en-1-one

Refernces