p-styryl-(p-tolyl)tin dichloride

Base Information

• Chemical Name: p-styryl-(p-tolyl)tin dichloride
• CAS No.: 74255-84-8
• Molecular Formula: C₁₅H₁₄Cl₂Sn
• Molecular Weight: 383.892
• Mol file: 74255-84-8.mol

Synonyms:

Chemical Property of p-styryl-(p-tolyl)tin dichloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-styryl-(p-tolyl)tin dichloride

There total 1 articles about p-styryl-(p-tolyl)tin dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-vinylbenzyl chloride (1073-67-2,24991-47-7) + magnesium (7439-95-4) + trichloro-4-tolylstannane (51353-34-5) → (p-styryl)di-p-tolyltin chloride (74255-82-6) + di-p-styryl-p-tolyltin chloride (74255-83-7) + di-p-tolyldi-p-styryltin(IV) (72611-66-6) + p-styryl-(p-tolyl)tin dichloride (74255-84-8)

Guidance literature:

With t-butylcatechol; HCl; In diethyl ether; pentane; byproducts: MgCl2; (Ar); Grignard soln. from Mg and styryl chloride was dropped to soln. of tin compd. within 1-1,5 h, t-butylcatechol was added and mixt. stirredovernight; solvent was removed in vac., residue taken up in toluene and treated with dild. HCl (ice-cooling), org. phases were concd. and sepd. by chromy.(silica gel, PE/diethyl ether); chloro tin compds. were not sepd., detected by NMR and IR;

DOI:10.1016/S0022-328X(00)93423-5

upstream raw materials:

4-vinylbenzyl chloride

magnesium

trichloro-4-tolylstannane

Refernces