di-p-styryl-p-tolyltin chloride

Base Information

Chemical Name:di-p-styryl-p-tolyltin chloride
CAS No.:74255-83-7
Molecular Formula:C₂₃H₂₁ClSn
Molecular Weight:451.583
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-p-styryl-p-tolyltin chloride

Chemical Property:

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Technology Process of di-p-styryl-p-tolyltin chloride

There total 2 articles about di-p-styryl-p-tolyltin chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.6%

: 1073-67-2,24991-47-7
4-vinylbenzyl chloride

: 32538-29-7
di(p-tolyl)tin dichloride

: 7439-95-4
magnesium

: 74255-82-6
(p-styryl)di-p-tolyltin chloride

: 74255-83-7
di-p-styryl-p-tolyltin chloride

: 72611-66-6
di-p-tolyldi-p-styryltin(IV)

Guidance literature:: With t-butylcatechol; HCl; In diethyl ether; pentane; byproducts: MgCl2; (Ar); Grignard soln. from Mg and styryl chloride was dropped to soln. of tin compd. within 1-1,5 h, t-butylcatechol was added and mixt. stirredovernight; solvent was removed in vac., residue taken up in toluene and treated with dild. HCl (ice-cooling), org. phases were concd. and sepd. by chromy.(silica gel, PE/diethyl ether); elem. anal.; chloro tin compds. were not sepd., detected by NMR;
DOI:10.1016/S0022-328X(00)93423-5

Reference yield:

: 1073-67-2,24991-47-7
4-vinylbenzyl chloride

: 7439-95-4
magnesium

: 51353-34-5
trichloro-4-tolylstannane

: 74255-82-6
(p-styryl)di-p-tolyltin chloride

: 74255-83-7
di-p-styryl-p-tolyltin chloride

: 72611-66-6
di-p-tolyldi-p-styryltin(IV)

: 74255-84-8
p-styryl-(p-tolyl)tin dichloride

Guidance literature:: With t-butylcatechol; HCl; In diethyl ether; pentane; byproducts: MgCl2; (Ar); Grignard soln. from Mg and styryl chloride was dropped to soln. of tin compd. within 1-1,5 h, t-butylcatechol was added and mixt. stirredovernight; solvent was removed in vac., residue taken up in toluene and treated with dild. HCl (ice-cooling), org. phases were concd. and sepd. by chromy.(silica gel, PE/diethyl ether); chloro tin compds. were not sepd., detected by NMR and IR;
DOI:10.1016/S0022-328X(00)93423-5