1,1,6,6-Tetramethyl-2,3,6,7-tetrahydro-1H,5H-benzo[ij]phosphinolizine oxide

Base Information

• Chemical Name: 1,1,6,6-Tetramethyl-2,3,6,7-tetrahydro-1H,5H-benzo[ij]phosphinolizine oxide
• CAS No.: 311806-51-6
• Molecular Formula: C₁₆H₂₃OP
• Molecular Weight: 262.332
• Mol file: 311806-51-6.mol

Synonyms:

Chemical Property of 1,1,6,6-Tetramethyl-2,3,6,7-tetrahydro-1H,5H-benzo[ij]phosphinolizine oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1,6,6-Tetramethyl-2,3,6,7-tetrahydro-1H,5H-benzo[ij]phosphinolizine oxide

There total 1 articles about 1,1,6,6-Tetramethyl-2,3,6,7-tetrahydro-1H,5H-benzo[ij]phosphinolizine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2-Hydroxy-3-methylbutyl)-4,4-dimethyl-1,2,3,4-tetrahydrophosphinoline oxide (311806-50-5) → (2-hydroxy-3-methylbutyl)methylphenylphosphine oxide (311806-48-1) + 1,4,4-trimethyl-1,2,3,4-tetrahydrophosphinoline-1-oxide (311806-49-2) + 1,1,6,6-Tetramethyl-2,3,6,7-tetrahydro-1H,5H-benzo[ij]phosphinolizine oxide (311806-51-6)

Guidance literature:

With PPA; at 120 ℃; for 120h; Title compound not separated from byproducts.;

DOI:10.1039/b004525j

upstream raw materials:

1-(2-Hydroxy-3-methylbutyl)-4,4-dimethyl-1,2,3,4-tetrahydrophosphinoline oxide