(Z)-2-(N-methylamino)-1-phenylethenyl isocyanide

Base Information

• Chemical Name: (Z)-2-(N-methylamino)-1-phenylethenyl isocyanide
• CAS No.: 173315-70-3
• Molecular Formula: C₁₀H₁₀N₂
• Molecular Weight: 158.203

Synonyms:

Chemical Property of (Z)-2-(N-methylamino)-1-phenylethenyl isocyanide

Chemical Property:

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Technology Process of (Z)-2-(N-methylamino)-1-phenylethenyl isocyanide

There total 3 articles about (Z)-2-(N-methylamino)-1-phenylethenyl isocyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.8%

1-methyl-4-phenyl-1H-pyrazole (10199-69-6) → N-methyl-4-phenylimidazole (2411-77-0) + (E)/(Z)-3-(N-methylamino)-2-phenylpropenenitrile (36758-69-7) + (Z)-2-(N-methylamino)-1-phenylethenyl isocyanide (173315-70-3)

Guidance literature:

In methanol; for 1h; Photolysis;

DOI:10.1021/jo970897r

Reference yield:

1-methyl-4-phenyl-1H-pyrazole (10199-69-6) → (Z)-3-(N-methylamino)-2-phenylpropenenitrile (70205-68-4) + (E)-3-(N-methylamino)-2-phenylpropenenitrile (70205-77-5) + (E)-2-(N-methylamino)-1-phenylethenyl isocyanide + (Z)-2-(N-methylamino)-1-phenylethenyl isocyanide (173315-70-3)

Guidance literature:

In methanol; for 1h; Further byproducts given. Yields of byproduct given; Irradiation;

DOI:10.1021/jo00130a011

Reference yield:

1-methyl-4-phenyl-1H-pyrazole (10199-69-6) → N-methyl-4-phenylimidazole (2411-77-0) + (Z)-3-(N-methylamino)-2-phenylpropenenitrile (70205-68-4) + (E)-3-(N-methylamino)-2-phenylpropenenitrile (70205-77-5) + (E)-2-(N-methylamino)-1-phenylethenyl isocyanide + (Z)-2-(N-methylamino)-1-phenylethenyl isocyanide (173315-70-3)

Guidance literature:

In methanol; for 3h; Product distribution; Mechanism; Irradiation; various pyrazoles;

DOI:10.1021/jo00130a011

upstream raw materials:

1-methyl-4-phenyl-1H-pyrazole

Downstream raw materials:

N-methyl-4-phenylimidazole

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