bis(3-methyl-1-m-tolyl-3-hydroxy-triazene-⁽¹⁾)-cobalt(II)

Base Information

Chemical Name:bis(3-methyl-1-m-tolyl-3-hydroxy-triazene-⁽¹⁾)-cobalt(II)
CAS No.:149478-68-2
Molecular Formula:C₁₆H₂₀CoN₆O₂
Molecular Weight:387.367
Hs Code.:

bis(3-methyl-1-m-tolyl-3-hydroxy-triazene-<sup>(1)</sup>)-cobalt(II)

Synonyms:

Suppliers and Price of bis(3-methyl-1-m-tolyl-3-hydroxy-triazene-⁽¹⁾)-cobalt(II)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(3-methyl-1-m-tolyl-3-hydroxy-triazene-⁽¹⁾)-cobalt(II)

Chemical Property:

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Technology Process of bis(3-methyl-1-m-tolyl-3-hydroxy-triazene-⁽¹⁾)-cobalt(II)

There total 2 articles about bis(3-methyl-1-m-tolyl-3-hydroxy-triazene-⁽¹⁾)-cobalt(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103521-40-0
3-hydroxy-3-methyl-1-(3'-tolyl)-1-triazene

: 71-48-7,917-69-1,5931-89-5,55881-15-7,68931-68-0,68931-69-1,93029-27-7
cobalt(II) acetate

: 149478-68-2,149564-50-1
bis(3-methyl-1-m-tolyl-3-hydroxy-triazene-⁽¹⁾)-cobalt(II)

Guidance literature:: In ethanol; formation from alc. soln. of 3-methyl-1-m-tolyl-3-hydroxy-triazene-(1) and Co(II) acetate in H2 atmosphere;; drying;;
DOI:10.1039/JR9380001346

Reference yield:

: 103521-40-0
3-hydroxy-3-methyl-1-(3'-tolyl)-1-triazene

: 6147-53-1
cobalt(II) diacetate tetrahydrate

: 149478-68-2,149564-50-1
bis(3-methyl-1-m-tolyl-3-hydroxy-triazene-⁽¹⁾)-cobalt(II)

Guidance literature:: In methanol; dissolving ligand in min. amt. of boiling aq. methanol in inert atmosphere; dropwise addn. of Co(CH3CO2)2*4H2O in degassed methanol;; filtration; washing with cooled degassed methanol; drying in vac.; elem. anal.;;
DOI:10.1039/DT9930001611