1,10-bis-(4-methoxy-phenyl)-decane-5,6-diol

Base Information

• Chemical Name: 1,10-bis-(4-methoxy-phenyl)-decane-5,6-diol
• CAS No.: 854401-87-9
• Molecular Formula: C₂₄H₃₄O₄
• Molecular Weight: 386.532
• Mol file: 854401-87-9.mol

Synonyms:

Chemical Property of 1,10-bis-(4-methoxy-phenyl)-decane-5,6-diol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,10-bis-(4-methoxy-phenyl)-decane-5,6-diol

There total 3 articles about 1,10-bis-(4-methoxy-phenyl)-decane-5,6-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(4-methoxyphenyl)pentanoic acid ethyl ester (79023-06-6) → 1,10-bis-(4-methoxy-phenyl)-decane-5,6-diol (854401-87-9)

Guidance literature:

With sodium; Petroleum ether; butan-1-ol; weiteres Reagens: Aethanol;

DOI:10.1080/00173130150503759

Reference yield:

5-(4-methoxyphenyl)pentanoic acid (7508-04-5) → 1,10-bis-(4-methoxy-phenyl)-decane-5,6-diol (854401-87-9)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol; sulfuric acid

2: petroleum ether; butanol-⁽¹⁾; sodium / weiteres Reagens: Aethanol

With ethanol; sulfuric acid; sodium; Petroleum ether; butan-1-ol;

DOI:10.1080/00173130150503759

Reference yield:

5-(4-methoxyphenyl)-5-oxopentanoic acid (4609-10-3) → 1,10-bis-(4-methoxy-phenyl)-decane-5,6-diol (854401-87-9)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol; amalgamated zinc; aqueous hydrochloric acid

2: ethanol; sulfuric acid

3: petroleum ether; butanol-⁽¹⁾; sodium / weiteres Reagens: Aethanol

With hydrogenchloride; amalgamated zinc; ethanol; sulfuric acid; sodium; Petroleum ether; butan-1-ol;

DOI:10.1080/00173130150503759

upstream raw materials:

5-(4-methoxyphenyl)pentanoic acid ethyl ester

5-(4-methoxyphenyl)pentanoic acid

5-(4-methoxyphenyl)-5-oxopentanoic acid

Downstream raw materials:

5-(4-methoxyphenyl)pentanoic acid

5-(4-methoxyphenyl)pentan-1-al