β-(acetoxymercurio)acetophenone

Base Information

Chemical Name:β-(acetoxymercurio)acetophenone
CAS No.:5653-24-7
Molecular Formula:C₁₀H₁₀HgO₃
Molecular Weight:378.778
Hs Code.:

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Suppliers and Price of β-(acetoxymercurio)acetophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β-(acetoxymercurio)acetophenone

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Technology Process of β-(acetoxymercurio)acetophenone

There total 2 articles about β-(acetoxymercurio)acetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1600-27-7
mercury(II) diacetate

: 536-74-3
phenylacetylene

: 5653-24-7
β-(acetoxymercurio)acetophenone

Guidance literature:: In methanol; byproducts: (C6H5CC)2Hg, C6H5C(OCH3)CHHgOC(O)CH3, C6H5COCH3; mercuric acetate in methanol added dropwise to a stirred soln. of ethynylbenzene at room temp. under N2, pptd., stirred for 1 h, further byproduct: C6H5C(OCH3)CH2; powder filtered off, washed with cold methanol, identified by iododemercuration as (PhCC)2Hg, solvent removed from the filtrate, filtered off (24 h later), washed with 40-70°C petroleum ether, identified as β-(acetoxymercurio)acetophenone;
DOI:10.1021/om00123a001