4,4'-ethylidene-di-benzoic acid bis-(2-ethyl-hexyl ester)

Base Information

• Chemical Name: 4,4'-ethylidene-di-benzoic acid bis-(2-ethyl-hexyl ester)
• CAS No.: 103512-53-4
• Molecular Formula: C₃₂H₄₆O₄
• Molecular Weight: 494.715
• Mol file: 103512-53-4.mol

Synonyms:

Chemical Property of 4,4'-ethylidene-di-benzoic acid bis-(2-ethyl-hexyl ester)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4'-ethylidene-di-benzoic acid bis-(2-ethyl-hexyl ester)

There total 4 articles about 4,4'-ethylidene-di-benzoic acid bis-(2-ethyl-hexyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-bis(4-chlorophenyl)ethane (3547-04-4) → 4,4'-ethylidene-di-benzoic acid bis-(2-ethyl-hexyl ester) (103512-53-4)

Guidance literature:

Multi-step reaction with 3 steps

1: quinoline

2: NaOH; aqueous ethylene glycol

3: H₂SO₄

With quinoline; sodium hydroxide; sulfuric acid; ethylene glycol;

DOI:10.1139/v56-056

Reference yield:

4,4'-ethylidene-di-benzonitrile (101290-87-3) → 4,4'-ethylidene-di-benzoic acid bis-(2-ethyl-hexyl ester) (103512-53-4)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOH; aqueous ethylene glycol

2: H₂SO₄

With sodium hydroxide; sulfuric acid; ethylene glycol;

DOI:10.1139/v56-056

Reference yield:

chlorobenzene (108-90-7) → 4,4'-ethylidene-di-benzoic acid bis-(2-ethyl-hexyl ester) (103512-53-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 1,1-diacetoxy-ethane; FSO₃H; HF

2: quinoline

3: NaOH; aqueous ethylene glycol

4: H₂SO₄

With quinoline; sodium hydroxide; ethylidene diacetate; sulfuric acid; hydrogen fluoride; fluorosulphonic acid; ethylene glycol;

DOI:10.1139/v56-056

upstream raw materials:

2-Ethylhexyl alcohol

4,4'-ethylidene-di-benzoic acid

1,1-bis(4-chlorophenyl)ethane

4,4'-ethylidene-di-benzonitrile