N-<3-butyl>-N-tosylamino>propyl>phthalimid

Base Information

• Chemical Name: N-<3-butyl>-N-tosylamino>propyl>phthalimid
• CAS No.: 134935-55-0
• Molecular Formula: C₂₅H₃₄N₄O₄S*ClH
• Molecular Weight: 523.096

Synonyms:

Chemical Property of N-<3-butyl>-N-tosylamino>propyl>phthalimid

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N-<3-butyl>-N-tosylamino>propyl>phthalimid

There total 3 articles about N-<3-butyl>-N-tosylamino>propyl>phthalimid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N1,4-Bis<(tert-butoxy)carbonyl>-N12-phthaloyl-9-tosylspermin (134935-54-9) → N-<3-butyl>-N-tosylamino>propyl>phthalimid (134935-55-0)

Guidance literature:

With hydrogenchloride;

DOI:10.1002/hlca.19910740322

Reference yield:

N-(N3-p-toluenesulfonyl)-3-aminopropylphthalimide (38353-77-4) → N-<3-butyl>-N-tosylamino>propyl>phthalimid (134935-55-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) Cs₂CO₃ / 1) toluene, 1 h, reflux, 2) toluene, 12 h, reflux

2: aq. HCl

With hydrogenchloride; caesium carbonate;

DOI:10.1002/hlca.19910740322

Reference yield:

O,O'-Di(tert-butyl)-N-<4-(mesyloxy)butyl>-N,N'-(propan-1,3-diyl)bis (134935-53-8) → N-<3-butyl>-N-tosylamino>propyl>phthalimid (134935-55-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) Cs₂CO₃ / 1) toluene, 1 h, reflux, 2) toluene, 12 h, reflux

2: aq. HCl

With hydrogenchloride; caesium carbonate;

DOI:10.1002/hlca.19910740322

upstream raw materials:

N¹,4-Bis<(tert-butoxy)carbonyl>-N¹²-phthaloyl-9-tosylspermin

N-(N³-p-toluenesulfonyl)-3-aminopropylphthalimide

O,O'-Di(tert-butyl)-N-<4-(mesyloxy)butyl>-N,N'-(propan-1,3-diyl)bis

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