α-carbonylpiperidine-o-hydroxycinnamic acid piperidide

Base Information

• Chemical Name: α-carbonylpiperidine-o-hydroxycinnamic acid piperidide
• CAS No.: 77509-73-0
• Molecular Formula: C₂₀H₂₆N₂O₃
• Molecular Weight: 342.438
• Mol file: 77509-73-0.mol

Synonyms:

Chemical Property of α-carbonylpiperidine-o-hydroxycinnamic acid piperidide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-carbonylpiperidine-o-hydroxycinnamic acid piperidide

There total 4 articles about α-carbonylpiperidine-o-hydroxycinnamic acid piperidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

piperidine (110-89-4) + coumarin-3-carbonylpiperidine (18144-51-9) → α-carbonylpiperidine-o-hydroxycinnamic acid piperidide (77509-73-0)

Guidance literature:

for 6h; Heating;

DOI:10.1002/jhet.5570180122

Reference yield:

piperidine (110-89-4) → α-carbonylpiperidine-o-hydroxycinnamic acid piperidide (77509-73-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / 0.17 h / heating on water bath

2: 55 percent / 6 h / Heating

DOI:10.1002/jhet.5570180122

Reference yield:

coumarin 3-carboxylic acid chloride (3757-06-0) → α-carbonylpiperidine-o-hydroxycinnamic acid piperidide (77509-73-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / 0.17 h / heating on water bath

2: 55 percent / 6 h / Heating

DOI:10.1002/jhet.5570180122

upstream raw materials:

piperidine

coumarin-3-carbonylpiperidine

coumarin 3-carboxylic acid chloride

2-oxo-2H-chromene-3-carboxylic acid