dimethyl ethyl (2-methyl-4-phenyl)but-2-yl ammonium iodide

Base Information

• Chemical Name: dimethyl ethyl (2-methyl-4-phenyl)but-2-yl ammonium iodide
• CAS No.: 79399-14-7
• Molecular Formula: C₁₅H₂₆N*I
• Molecular Weight: 347.283
• Mol file: 79399-14-7.mol

Synonyms:

Chemical Property of dimethyl ethyl (2-methyl-4-phenyl)but-2-yl ammonium iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dimethyl ethyl (2-methyl-4-phenyl)but-2-yl ammonium iodide

There total 1 articles about dimethyl ethyl (2-methyl-4-phenyl)but-2-yl ammonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[1,1-dimethyl-3-phenylpropyl]acetamide (79399-13-6) + methyl iodide (74-88-4) → dimethyl ethyl (2-methyl-4-phenyl)but-2-yl ammonium iodide (79399-14-7)

Guidance literature:

With lithium aluminium tetrahydride; Yield given. Multistep reaction; 1) ether, 2) MeOH, r.t., 12 h;

DOI:10.1016/S0040-4020(01)92018-6

Reference yield:

dimethyl ethyl (2-methyl-4-phenyl)but-2-yl ammonium iodide (79399-14-7) → 3-methyl-1-phenylbut-2-ene (4489-84-3) + 2-methyl-4-phenyl-1-butene (6683-51-8)

Guidance literature:

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; at 19 ℃; for 24h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1016/S0040-4020(01)92018-6

upstream raw materials:

N-[1,1-dimethyl-3-phenylpropyl]acetamide

methyl iodide

Downstream raw materials:

3-methyl-1-phenylbut-2-ene

2-methyl-4-phenyl-1-butene