2-Dibromomethyl-benzoic acid (2R,3R,4R,5R)-3-[(2-chloro-phenoxy)-hydroxy-phosphoryloxy]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-(4-methoxy-tetrahydro-pyran-4-yloxy)-tetrahydro-furan-2-ylmethyl ester; compound with triethyl-amine

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Chemical Name:2-Dibromomethyl-benzoic acid (2R,3R,4R,5R)-3-[(2-chloro-phenoxy)-hydroxy-phosphoryloxy]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-(4-methoxy-tetrahydro-pyran-4-yloxy)-tetrahydro-furan-2-ylmethyl ester; compound with triethyl-amine
CAS No.:77451-39-9
Molecular Formula:C₆H₁₅N*C₂₉H₃₀Br₂ClN₂O₁₂P
Molecular Weight:925.99
Hs Code.:

2-Dibromomethyl-benzoic acid (2R,3R,4R,5R)-3-[(2-chloro-phenoxy)-hydroxy-phosphoryloxy]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-(4-methoxy-tetrahydro-pyran-4-yloxy)-tetrahydro-furan-2-ylmethyl ester; compound with triethyl-amine

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Chemical Property of 2-Dibromomethyl-benzoic acid (2R,3R,4R,5R)-3-[(2-chloro-phenoxy)-hydroxy-phosphoryloxy]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-(4-methoxy-tetrahydro-pyran-4-yloxy)-tetrahydro-furan-2-ylmethyl ester; compound with triethyl-amine

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Technology Process of 2-Dibromomethyl-benzoic acid (2R,3R,4R,5R)-3-[(2-chloro-phenoxy)-hydroxy-phosphoryloxy]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-(4-methoxy-tetrahydro-pyran-4-yloxy)-tetrahydro-furan-2-ylmethyl ester; compound with triethyl-amine

There total 3 articles about 2-Dibromomethyl-benzoic acid (2R,3R,4R,5R)-3-[(2-chloro-phenoxy)-hydroxy-phosphoryloxy]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-(4-methoxy-tetrahydro-pyran-4-yloxy)-tetrahydro-furan-2-ylmethyl ester; compound with triethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73407-51-9
o-di-bromomethyl-benzoyl chloride

: 77451-39-9
2-Dibromomethyl-benzoic acid (2R,3R,4R,5R)-3-[(2-chloro-phenoxy)-hydroxy-phosphoryloxy]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-(4-methoxy-tetrahydro-pyran-4-yloxy)-tetrahydro-furan-2-ylmethyl ester; compound with triethyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / acetonitrile; pyridine / Ambient temperature

In pyridine; acetonitrile;
DOI:10.1016/0040-4020(80)88035-5

Reference yield:

: 17327-23-0
2'-O-(tetrahydro-4-methoxy-2H-pyran-4-yl)uridine

: 77451-39-9
2-Dibromomethyl-benzoic acid (2R,3R,4R,5R)-3-[(2-chloro-phenoxy)-hydroxy-phosphoryloxy]-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-4-(4-methoxy-tetrahydro-pyran-4-yloxy)-tetrahydro-furan-2-ylmethyl ester; compound with triethyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / acetonitrile; pyridine / Ambient temperature

In pyridine; acetonitrile;
DOI:10.1016/0040-4020(80)88035-5