{WN(N(C₆H₅)2)3}

Base Information

Chemical Name:{WN(N(C₆H₅)2)3}
CAS No.:136427-40-2
Molecular Formula:C₃₆H₃₀N₄W
Molecular Weight:702.511
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {WN(N(C₆H₅)2)3}

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Technology Process of {WN(N(C₆H₅)2)3}

There total 2 articles about {WN(N(C₆H₅)2)3} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.3%

: 109-72-8,29786-93-4
n-butyllithium

: 14259-69-9
tungsten nitride trichloride

: 122-39-4
diphenylamine

: 136427-40-2
{WN(N(C₆H₅)2)3}

Guidance literature:: In tetrahydrofuran; hexane; byproducts: LiCl; a soln. of n-BuLi in hexane was added to NHPh2 in THF at 0°C under Ar, stirred for 30 min, the soln. was added dropwise to WNCl3 in THF at -45°C, stirred for 3 h while warming to room temp.; filtn. (LiCl), concn.; elem. anal.;

Reference yield: 3.1%

: 109-72-8,29786-93-4
n-butyllithium

: 14259-69-9
tungsten nitride trichloride

: 122-39-4
diphenylamine

: 136427-40-2
{WN(N(C₆H₅)2)3}

: {W₄N₄(N(C₆H₅)2)6(OCH₂CH₂CH₂CH₃)2}

Guidance literature:: In tetrahydrofuran; hexane; byproducts: LiCl; an excess of n-BuLi in hexane was added to NHPh2 in THF at 0°C under Ar, the soln. was added dropwise to WNCl3 in THF at -45°C, stirred for 3 h while warming to room temp.; filtn. (LiCl), concn., allowed to stand for 3 weeks, crystn., crystals were filtered off and dried in an Ar stream; elem. anal.;