(C₆H₅)3SnCCCH₂OCH₂CHCH₂

Base Information

• Chemical Name: (C₆H₅)3SnCCCH₂OCH₂CHCH₂
• CAS No.: 329200-85-3
• Molecular Formula: C₂₄H₂₂OSn
• Molecular Weight: 445.148
• Mol file: 329200-85-3.mol

Synonyms:

Chemical Property of (C₆H₅)3SnCCCH₂OCH₂CHCH₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (C₆H₅)3SnCCCH₂OCH₂CHCH₂

There total 1 articles about (C₆H₅)3SnCCCH₂OCH₂CHCH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

allyl propargyl ether (51580-41-7) + triphenylstannylcobaloxime → (C6H5)3SnCCCH2OCH2CHCH2 (329200-85-3) + phenylcobaloxime (29130-85-6)

Guidance literature:

In acetonitrile; Irradiation (UV/VIS); mixt. of Co complex and enyne in acetonitrile, which was deaerated in ultrasonic bath with bubbling argon, was refluxed for 22 h under argon; condensed in vac.; residue was pass through column of Florisil (CH2Cl2);eluate was subjected to TLC sepn. (hexane-ethyl acetate, 10/1);

DOI:10.1016/S0022-328X(00)00550-7

upstream raw materials:

allyl propargyl ether