1,1-dimethyl-2-chloro-2,3,3-tris(2,4,6-triisopropylphenyl)disilastannirane

Base Information

• Chemical Name: 1,1-dimethyl-2-chloro-2,3,3-tris(2,4,6-triisopropylphenyl)disilastannirane
• CAS No.: 1228573-34-9
• Molecular Formula: C₄₇H₇₅ClSi₂Sn
• Molecular Weight: 850.447

Synonyms:

Chemical Property of 1,1-dimethyl-2-chloro-2,3,3-tris(2,4,6-triisopropylphenyl)disilastannirane

Chemical Property:

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Technology Process of 1,1-dimethyl-2-chloro-2,3,3-tris(2,4,6-triisopropylphenyl)disilastannirane

There total 1 articles about 1,1-dimethyl-2-chloro-2,3,3-tris(2,4,6-triisopropylphenyl)disilastannirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

Tip2Si=Si(Tip)Li + dimethyltin dichloride (753-73-1) → 1,1-dimethyl-2-chloro-2,3,3-tris(2,4,6-triisopropylphenyl)disilastannirane (1228573-34-9)

Guidance literature:

In toluene; (Ar or N2); Schlenk techniques; toluene soln. of disilenide deriv. addeddropwise to a soln. of Me2SnCl2 over a period of 15 min at room temp.; stirred overnight at room temp.; filtered off; evapn.; crystd. from hexane at o°C; detn. by NMR, MS;

DOI:10.1002/zaac.200900234

upstream raw materials:

dimethyltin dichloride

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