MoO₂(S₂P(OC₆H₅)2)2

Base Information

Chemical Name:MoO₂(S₂P(OC₆H₅)2)2
CAS No.:150485-46-4
Molecular Formula:C₂₄H₂₀MoO₆P₂S₄
Molecular Weight:690.571
Hs Code.:

MoO<sub>2</sub>(S<sub>2</sub>P(OC<sub>6</sub>H<sub>5</sub>)2)2

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of MoO₂(S₂P(OC₆H₅)2)2

Chemical Property:

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Technology Process of MoO₂(S₂P(OC₆H₅)2)2

There total 3 articles about MoO₂(S₂P(OC₆H₅)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: {Mo₂O₃(S₂P(OC₆H₅)2)4}

: 150485-46-4
MoO₂(S₂P(OC₆H₅)2)2

: 25395-93-1
{MoO(S₂P(OC₆H₅)2)2}

Guidance literature:: In toluene; Irradiation (UV/VIS); photodissociation of starting material in toluene at 30°C illuminated with a 200 Watt Hg-Xe arclamp (510 nm); monitored by UV-spectroscopy;

Reference yield:

: 2253-60-3
O,O-diphenyl phosphorodithioic acid

: 108-95-2,27073-41-2
phenol

: 150485-46-4
MoO₂(S₂P(OC₆H₅)2)2

: 25395-93-1
{MoO(S₂P(OC₆H₅)2)2}

Guidance literature:: Multi-step reaction with 2 steps

1: melt

2: toluene

In toluene;

Reference yield:

: 2253-60-3
O,O-diphenyl phosphorodithioic acid

: bis(acetylacetonato)dioxomolybenum(VI)

: 150485-46-4
MoO₂(S₂P(OC₆H₅)2)2

: Mo₂O₃(S₂P(OC₆H₅)2)4

Guidance literature:: In methanol; byproducts: dithiophosphoryl disulphide; precautions were taken to exclude moisture; react. in 1:2 molar ratio of MoO2(acac)2 with the corresponding dithiophosphoric acid in CH3OH at 0-5°C, stirring of react. soln. for 1 h; filtration of ppt., washing with CH3OH, then n-hexane, drying in vac., recrystn. from benzene-n-hexane (1:1); elem. anal.;
DOI:10.1016/S0020-1693(00)83101-1