fac-bis(diphenylphosphino)(trimethylsilyl)methylmanganese tricarbonyl

Base Information

• Chemical Name: fac-bis(diphenylphosphino)(trimethylsilyl)methylmanganese tricarbonyl
• CAS No.: 114762-77-5
• Molecular Formula: C₃₁H₂₉MnO₃P₂Si
• Molecular Weight: 594.54
• Mol file: 114762-77-5.mol

Synonyms:

Chemical Property of fac-bis(diphenylphosphino)(trimethylsilyl)methylmanganese tricarbonyl

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of fac-bis(diphenylphosphino)(trimethylsilyl)methylmanganese tricarbonyl

There total 1 articles about fac-bis(diphenylphosphino)(trimethylsilyl)methylmanganese tricarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pentacarbonyl(methyl)manganese(I) + 2,2-dimethyl-2-sila-1,3-bis(diphenylphosphino)propane (59557-18-5) → fac-bis(diphenylphosphino)(trimethylsilyl)methylmanganese tricarbonyl (114762-77-5)

Guidance literature:

In toluene; byproducts: CH4, CO; The mixture in dry toluene is heated at reflux under N2 for 12 h.; The light brown reaction mixture is filtered to yield a clear yellow-green soln., dry hexane is added to the soln. and upon standing overnight yielded a crystalline complex, elem. anal.;

upstream raw materials:

2,2-dimethyl-2-sila-1,3-bis(diphenylphosphino)propane