tris[trimethylsilyl)silyl]zinc chlorideTMEDAtoluene

Base Information

Chemical Name:tris[trimethylsilyl)silyl]zinc chloride*TMEDA*toluene
CAS No.:1219010-85-1
Molecular Formula:C₇H₈*C₁₅H₄₃ClN₂Si₄Zn
Molecular Weight:556.845
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris[trimethylsilyl)silyl]zinc chloride*TMEDA*toluene

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Technology Process of tris[trimethylsilyl)silyl]zinc chloride*TMEDA*toluene

There total 1 articles about tris[trimethylsilyl)silyl]zinc chloride*TMEDA*toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 4098-98-0
tetrakis(trimethylsilyl)silane

: 7646-85-7,24359-56-6
zinc(II) chloride

: 1219010-85-1
tris[trimethylsilyl)silyl]zinc chloride*TMEDA*toluene

Guidance literature:: With KOC(CH₃)3; In toluene; (inert atm.); to soln. of silane in toluene KO(t)Bu and TMEDA were added, stirred for 5 d, evapd. in vac., dissolved in toluene, ZnCl2 was added, stirred for 60 min; filtered, evapd. in vac, crystd. from pentane soln. at -70°C;
DOI:10.1039/b910463a