meso-diphenylbisanthene

Base Information

• Chemical Name: meso-diphenylbisanthene
• CAS No.: 23102-66-1
• Molecular Formula: C₄₀H₂₂
• Molecular Weight: 502.615
• Mol file: 23102-66-1.mol

Synonyms:

Chemical Property of meso-diphenylbisanthene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of meso-diphenylbisanthene

There total 6 articles about meso-diphenylbisanthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7,14-diphenyl-7,14-dihydro-phenanthro[1,10,9,8-opqra]perylene-7,14-diol (872810-09-8) → meso-diphenylbisanthene (23102-66-1)

Guidance literature:

With sodium hypophosphite; acetic acid; potassium iodide; Erhitzen des Reaktionsprodukts mit PbO unter vermindertem Druck auf 360grad;

Reference yield:

7,14-diethoxy-7,14-diphenyl-7,14-dihydro-phenanthro[1,10,9,8-opqra]perylene → meso-diphenylbisanthene (23102-66-1)

Guidance literature:

With sodium hypophosphite; acetic acid; potassium iodide; Erhitzen des Reaktionsprodukts mit PbO unter vermindertem Druck auf 360grad;

Reference yield:

phenyllithium (591-51-5) → meso-diphenylbisanthene (23102-66-1)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: NaH₂PO₂; KI; glacial acetic acid / Erhitzen des Reaktionsprodukts mit PbO unter vermindertem Druck auf 360grad

With sodium hypophosphite; diethyl ether; acetic acid; potassium iodide;

upstream raw materials:

7,14-diphenyl-7,14-dihydro-phenanthro[1,10,9,8-opqra]perylene-7,14-diol

acetic acid

10,10'-diphenyl-9,9'-bianthracene

phenyllithium